This paper aims to provide an overview concerning the optically stimulated luminescence OSL dating method and its applications for geomorphological research in France. An outline of the general physical principles of luminescence dating is given. A case study of fluvial sands from the lower terrace of the Moselle valley is then presented to describe the range of field and laboratory procedures required for successful luminescence dating. The paper also reviews the place of OSL dating in geomorphological research in France and assesses its potential for further research, by focusing on the diversity of sedimentary environments and topics to which it can be usefully applied. Hence it underlines the increasing importance of the method to geomorphological research, especially by contributing to the development of quantitative geomorphology. They are now largely used to date not only palaeontological or organic remains, but also minerals that characterise detrital clastic sedimentary material. The most common methods applied to minerals are cosmogenic radionuclides, electron spin resonance ESR and luminescence techniques. The latter were first applied to burned minerals from archaeological artefacts [thermoluminescence TL method].
Optically Stimulated Luminescence
Optical : Relating to the use of visible or near-visible light. Stimulated : To excite with a stimulus light or heat. Optically stimulated luminescence : The emission of light from crystalline materials when stimulated by light following previous absorption of energy from radiation. Luminescence dating consists of a family of analytical methods, most of which are used in archaeological research. They can be applied to samples ranging in age from just a few years to several hundreds of thousands of years beyond the range of radiocarbon dating , and they are, therefore, able to cover a time interval that includes important turning points in the evolution of humans.
as luminescence, and is dependent in various ways on whether TL, optically stimulated lu- minescence (OSL), etc., is used as the stimula- tion method.
Dating techniques of interest to archaeologists include thermoluminescence, optically stimulated luminescence, electron spin resonance, and fission track dating, as well as techniques that depend on annual bands or layers, such as dendrochronology , tephrochronology , and varve chronology. Single Quartz OSL ages can be determined typically from to , years BP, and can be reliable when suitable methods are used and proper checks are done.
Optical dating using Optically stimulated luminescence OSL has been used on sediments. In multiple-aliquot testing, a number of grains of sand are stimulated at the same time and the resulting luminescence signature is averaged. In contrast to the multiple-aliquot method, the Single-aliquot-regenerative-dose SAR method tests the burial ages of individual grains of sand which are then plotted. Mixed deposits can be identified and taken into consideration when determining the age .
Infrared stimulated luminescence IRSL dating of potassium feldspars has been used. Feldspar IRSL techniques have the potential to extend the datable range out to a million years as feldspars typically have significantly higher dose saturation levels than quartz, though issues regarding anomalous fading will need to be dealt with first.
The possible role of environmental change, especially sea level change, as a stimulus for the development of human residence and migration is poorly understood. We investigate this problem by showing a record of sea-level change and coastal transformation based on a sediment core FN1 core and a Neolithic site Pingfengshan site obtained from the Funing bay on the northeast coast of Fujian, China. Samples from FN1 core and Pingfengshan site were taken for grain size ananlyses and for optically stimulated luminescence OSL dating.
archaeology has recently been supplemented by optical dating methods. Optically stimulated lumi- nescence (OSL, using green or green/blue wave- lengths for.
Crystalline rock types and soils collect energy from the radioactive decay of cosmic uranium, thorium, and potassium Electrons from these substances get trapped in the mineral’s crystalline structure, and continuing exposure of the rocks to these elements over time leads to predictable increases in the number of electrons caught in the matrices. But when the rock is exposed to high enough levels of heat or light, that exposure causes vibrations in the mineral lattices and the trapped electrons are freed.
Luminescence dating is a collective term for dating methods that encompass thermoluminescence TL and optically stimulated luminescence OSL dating techniques. OSL is also less commonly referred to as optical dating, photon stimulated luminescence dating or photoluminescence dating.. Luminescence dating methods are based on the ability of some mineral grains to absorb and store energy from environmental ionizing radiation emanating from the immediate surroundings of the mineral grains as well as from cosmic radiation.
When stimulated these minerals, generally referred to as dosimeters, will release the stored energy in the form of visible light; hence the term luminescence. Measuring the energy and determining the rate at which the energy accumulated allows an age representing the time that has elapsed since the energy began accumulating to be determined.
Stimulation of energy release using heat is termed TL while stimulation using light is referred to as OSL. The age range of luminescence methods generally spans from a few decades to about , years, though ages exceeding several hundred thousand years have been reported in some studies.
Luminescence Dating Laboratory
Introduction How do we measure the OSL signal? How do we measure the radiation dose rate? Another way of dating glacial landforms is optically stimulated luminescence dating OSL. OSL is used on glacial landforms that contain sand, such as sandur or sediments in glacial streams.
With the assistance of Fugro LABORATORY we have developed a method for A polymineral single-aliquot osl for optically-stimulated luminescence dating.
Up to now not a single dating technique has been developed for in-situ planetary exploration. The only information on the age of extraterrestrial planetary surfaces comes from the “crater-counting” method. This method has an inherent large error and low resolution and is completely inadequate for local geology. Luminescence dating has possibly the potential to open up a completely new discipline in planetary in-situ exploration. This assessment has a strategic value for the development of a new generation of in-situ instrumentation.
Sedimentation processes on Mars are completely unexplored. In addition, fluid phases may have contributed significantly to erosion and transport processes to form the Martian landscape. Dating of buried grains in sedimentary layers would give a crucial contribution to the understanding of surface forming processes and is essential for any further exploration of planet Mars. It is therefore essential to develop a method, which can determine the chronology of sedimentary deposits.
Such a technique must be incorporated into an instrument requiring low resources mass, power, volume and placed onto the surface of Mars.
Testing Luminescence Dating Methods for Small Samples from Very Young Fluvial Deposits
Over the last 60 years, luminescence dating has developed into a robust chronometer for applications in earth sciences and archaeology. The technique is particularly useful for dating materials ranging in age from a few decades to around ,—, years. In this chapter, following a brief outline of the historical development of the dating method, basic principles behind the technique are discussed. This is followed by a look at measurement equipment that is employed in determining age and its operation.
Luminescence properties of minerals used in dating are then examined after which procedures used in age calculation are looked at. Sample collection methods are also reviewed, as well as types of materials that can be dated.
In , they also developed optically stimulated luminescence dating techniques, which use laser light, to date sediments. How does Luminescence work?
Optically-Stimulated Luminescence is a late Quaternary dating technique used to date the last time quartz sediment was exposed to light. As sediment is transported by wind, water, or ice, it is exposed to sunlight and zeroed of any previous luminescence signal. Once this sediment is deposited and subsequently buried, it is removed from light and is exposed to low levels of natural radiation in the surrounding sediment.
Through geologic time, quartz minerals accumulate a luminescence signal as ionizing radiation excites electrons within parent nuclei in the crystal lattice. A certain percent of the freed electrons become trapped in defects or holes in the crystal lattice of the quartz sand grain referred to as luminescent centers and accumulate over time Aitken, In our laboratory, these sediments are exposed to an external stimulus blue-green light and the trapped electrons are released.
The released electrons emit a photon of light upon recombination at a similar site. In order to relate the luminescence given off by the sample to an age, we first need to obtain the dose equivalent to the burial dose. Following the single-aliquot regenerative SAR method of Murray and Wintle , the dose equivalent De is calculated by first measuring the natural luminescence of a sample. Then, the bleached sample is given known laboratory doses of radiation, referred to as regenerative doses.
The regenerative dose data are fit with a saturating exponential to generate a luminescence dose-response curve. The De is calculated by the intercept of the natural luminescence signal with the generated curve. A curve is generated for each aliquot subsample , multiple aliquots are needed to obtain an accurate De. Murray, A.
Luminescence and ESR Dating
Luminescence dating including thermoluminescence and optically stimulated luminescence is a type of dating methodology that measures the amount of light emitted from energy stored in certain rock types and derived soils to obtain an absolute date for a specific event that occurred in the past. The method is a direct dating technique , meaning that the amount of energy emitted is a direct result of the event being measured.
In other words, OSL/IRSL is by default a destructive-readout technique where the trapped electron population decreases over the stimulation time because of their.
In physics , optically stimulated luminescence OSL is a method for measuring doses from ionizing radiation. It is used in at least two applications:. The method makes use of electrons trapped between the valence and conduction bands in the crystalline structure of certain minerals most commonly quartz and feldspar. The ionizing radiation produces electron-hole pairs: Electrons are in the conduction band and holes in the valence band.
The electrons that have been excited to the conduction band may become entrapped in the electron or hole traps. Under the stimulation of light, the electrons may free themselves from the trap and get into the conduction band. From the conduction band, they may recombine with holes trapped in hole traps.
Please reference: Mallinson, D. Optically stimulated luminescence is a method of determining the age of burial of quartz or feldspar bearing sediments based upon principles of radiation and excitation within crystal lattices, and stems from the fact that imperfections in a crystal lattice have the ability to store ionizing energy Aitken , ; Botter -Jensen et al. Radiation within sediments comes from alpha, beta, and gamma radiation emitted during the decay of U, U, Th, 40 K, and 87 Rb, and their daughter products, both within the mineral grains and in their surroundings Lian , , and from cosmic rays Figure 1.
Under controlled laboratory conditions, assuming the sample was collected under light-restricted conditions, controlled exposure of the sample to photons yields a luminescence response the equivalent dose, D e , the intensity of which is a function of the dose rate within the sediment, and the length of time the sample was exposed to the background radiation. In order to measure the age, two factors must be known; 1 the environmental dose rate, and 2 the laboratory dose of radiation that produces the same intensity of luminescence as did the environmental radiation dose the equivalent dose.
Luminescence dating is a well-established method of absolute chronology that They showed that there can be sufficient light penetration for OSL dating to be.
Optically Stimulated Luminescence OSL dating has emerged within the last 20 years as a key Quaternary absolute dating tool, with a wide range of terrestrial and marine applications. Optical dating techniques employ ubiquitous quartz or feldspar grains to directly date the deposition of sedimentary units. As such, the optical dating methods allow the systematic chronological evaluation of Quaternary-age sedimentary sequences. Within the School of Geography and the Environment, the OLD Laboratory provides support particularly for the Landscape Dynamics research cluster, with a specific focus on low latitude environment and climate change, geoarchaeology and geomorphology.
In addition our researchers continuously engage in efforts to improve and develop the methodology and to further advance our knowledge on the fundamental physical mechanisms underlying the dating method. The OLD Laboratory also provides a commercial luminescence dating service and works closely with clients in industry, archaeological organizations, environmental institutes and other academic groups. For commercial enquiries please contact Dr Szilvia Bajkan in the first instance clearly stating the following information:.
Depositional context of material e. Region from which samples are derived. If known, approximate estimate of age e. Timeframe of project i. Any other relevant information.
School of Geography and the Environment, University of Oxford
The DRI E. The DRILL is a research laboratory dedicated to fundamental investigations in the luminescence properties of earth materials, and to the application of luminescence dating techniques to geomorphological, geological, and archeological problems. The DRILL welcomes collaboration with research institute and university faculty, consultants, and government agency researchers.
most methods used for dating with quartz. Optically stimulated luminescence. (OSL). A second means of releasing the electrons. stored within minerals is by.
Optically stimulated luminescence dating at Rose Cottage Cave. A single-grain analysis demonstrates that the testing procedure for feldspar fails to reject single aliquots containing feldspar and the overestimate of age is attributed to this. Seven additional luminescence dates for the Middle Stone Age layers combined with the 14 C chronology establish the terminal Middle Stone Age deposits at 27 years ago, while stone tool assemblages that are transitional between the Middle Stone Age and the Late Stone Age are dated to between 27 years and 20 years ago.
Although there are inconsistencies in the Middle Stone Age dates, the results suggest that the Howiesons Poort at Rose Cottage Cave dates to between 70 years and 60 years ago. Much of the rich archaeological heritage in southern Africa is older than 50 years, which is the limit of the ubiquitous 14 C dating technique. In order to make appropriate inter-site comparisons of artefactual evidence, and further to compare the trajectory of human adaptation with external factors such as changing climates, it is necessary to establish a reliable chronological framework.
Optically stimulated luminescence OSL dating has become one of the foremost techniques in establishing this framework. OSL is based on the build-up and release of radiation energy in crystalline minerals, typically quartz. The charge build-up manifests as electrons, mobilized in the quartz matrix by environmental radiation, which populate pre-existing energy minima that are called ‘traps’.
OSL dates represent the time since electron traps within the quartz grains were previously emptied or bleached by heating or exposure to sunlight.